Description of experiment
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experiment.
Needed compounds: ----------------- sodium hydroxide : NaOH vanadium pentoxide : V2O5
Class: ------ elem=V precipitation
Summary: -------- Vanadium pentoxide can be dissolved in very concentrated solutions of NaOH in considerable quantities. When such a solution is cooled down, then a white crystalline solid separates from the liquid and the liquid completely solidifies.
Description: ------------ Adda fairly large amount of V2O5 to a concentrated solution of NaOH and heat until boiling: The solid quickly dissolves. The liquid does not become completely clear. (This may also be due to impurities in the V2O5).
Let liquid cool down: In the liquid, white spots appear at random places. These white spots slowly become larger and needle-like structures are formed, pointing in many directions, starting from the white spots. Finally, the complete liquid is filled by the needle-like crystal structures and the liquid has become solid.
Add some water to the solidified liquid and shake: The solid quickly breaks down in smaller particles and most of these particles dissolve.
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