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Experiments for 'thionyl chloride'
Below follows a summary of all experiments, matching your
search. Click one of the EXPERIMENT hyperlinks for a complete description of the
experiment.
Results for 'thionyl chloride':
EXPERIMENT 1 --------------- Thionyl chloride quickly hydrolyses in the presence of water.
EXPERIMENT 2 --------------- Iodide ion reacts with thionyl chloride, most likely giving iodine, and some sulphur(II) species. Potassium bromide does not dissolve in thionyl chloride (at least, not visibly). No reaction occurs.
EXPERIMENT 3 --------------- Potassium dichromate is sparingly soluble in thionyl chloride, giving an intensely colored red/orange/brown solution, which on addition to water at once becomes green with a blue hue. Potassium chromate does not dissolve in thionyl chloride. The solid changes color from yellow to yellow/orange, and the solution becomes slightly colored, but this faint reaction may be due to minor impurities in the potassium chromate or thionyl chloride. If any potassium chromate dissolves, then it is a very small amount.
EXPERIMENT 4 --------------- Thionyl chloride is not soluble in concentrated sulphuric acid, or only sparingly soluble. The mix of thionyl chloride and sulphuric acid is capable of forming chromyl chloride from potassium dichromate.
EXPERIMENT 5 --------------- Niobium pentachloride is soluble in thionyl chloride, but not very well. Also, such a solution becomes turbid.
EXPERIMENT 6 --------------- Iodine dissolves in thionyl chloride. It does not react. It gives a purple solution, looking very similar to a purple solution of iodine in an alkane or chlorinated hydrocarbons.
When water is added, then a remarkable reaction occurs. Sulphur is formed.
EXPERIMENT 7 --------------- Triethylamine frequently is used in reactions, where thionyl chloride is used, in order to capture any HCl formed in the reaction. However, when the only reactive compounds are thionyl chloride and triethylamine, then these two compounds react by themselves, giving rise to formation of black material, which sticks to the glass and is difficult to remove.
EXPERIMENT 8 --------------- Vanadium pentoxide does not dissolve in thionyl chloride, but when a small amount of water is added, then it reacts. Vanadium pentoxide dissolves in acetyl chloride, giving a dark red/brown solution.
EXPERIMENT 9 --------------- Thionyl chloride and copper nitrate react with each other, giving gaseous products and solid anhydrous copper(II) chloride remains behind.
EXPERIMENT 10 --------------- Formic acid does not form an acid chloride with thionylchloride, but it decomposes. Normally, the following reaction occurs:
RCOOH + SOCl2 --> RCOCl + SO2 + HCl
When R = H (formic acid), then decomposition occurs and carbon monoxide is formed.
End of results for 'thionyl chloride'
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